Glassy Carbon Round Robin

2009-07-20T13:51:32Z

Malfois:

==Samples==
Two samples of glassy carbons (labeled C4 and G9) from Jan Ilavsky have made their way (as of Dec 1 2008) to NIST, ILL and ISIS and will head on to Diamond and APS. Additionally another sample, labeled G8, has been measured at ISIS.

The samples are cut from glassy carbon material, manufactured by Alpha Aesar under description: Glassy Carbon type 2. These samples are manufactured in 50 x 50 mm plates, nominally 1 mm thick. Measurements with a micrometer were all between 0.99 and 1.01 mm

==Experimental details and Data==

===NIST===

<Gallery caption="NIST data for C4 and G9" widths="300px" heights="200px">
Image:C4.jpg|C4
Image:G9.jpg|G9
</Gallery>

Zip file of all data (in NIST 6 column format) with plots in PDF and Igor Pro formats [[Media:GlassyCarbon_NIST.zip|GlassyCarbon_NIST.zip]]

Zip file of all data (in canSAS XML 1D format) [[Media:GlassyCarbon_NIST_XML.zip|GlassyCarbon_NIST_XML.zip]]

===ILL===

<Gallery caption="ILL data for C4 and G9" widths="300px" heights="200px">
Image:C4_zoom.jpg|C4
Image:G9_zoom.jpg|G9
</Gallery>

Zip file of all data (in NIST 6 column format) with plots in PDF and Igor Pro formats [[Media:GlassyCarbon_ILL.zip|GlassyCarbon_ILL.zip]]

Zip file of all data (in canSAS XML 1D format) [[Media:GlassyCarbon_ILL_XML.zip|GlassyCarbon_ILL_XML.zip]]

===ISIS===

<Gallery caption="ISIS data for C4 and G9" widths="300px" heights="200px">
Image:LOQ_C4.jpg|C4
Image:LOQ_G9.jpg|G9
</Gallery>

The collected data in canSAS XML format : [[Media:GLASSYC_C4G8G9.XML‎|GLASSYC_C4G8G9.XML‎]] and in pseudo canSAS XML (includes T vs Lambda datasets): [[Media:GLASSYC_C4G8G9_withTL.XML‎|GLASSYC_C4G8G9_withTL.XML‎]]

Excel file of that data with plots : [[Media:Glassy_Carbons_C4_G8_G9.xls‎|Glassy_Carbons_C4_G8_G9.xls‎]]

===APS USAXS===

<Gallery caption="APS data for C4 and G9" widths="300px" heights="200px">
Image:C4_APS.jpg|C4
Image:G9_APS.jpg|G9
</Gallery>

Zip file of all data (in ASCII 3 column format) with plots in PDF and Igor Pro formats [[Media:GlassyCarbon_APS.zip|GlassyCarbon_APS.zip]]

Zip file of all data (in canSAS XML 1D format) [[Media:GlassyCarbon_APS_XML.zip|GlassyCarbon_APS_XML.zip]]

===ESRF ID01 PINHOLE===

The calibration sample measured on ID01 is designated "Glassy Carbon type 2 C, sample C14", thickness 1 mm.

The scattering intensity has been determined by cross calibration with a secondary standard ("lupolen BL4"). The
scattering intensity of this sample decreases locally with the absorbed dose where irradiated. The unirradiated parts of
this sample have identical scattering intensities that are higher than the scattering intensites of the irradiated parts.
The calibration factor was found by scanning the secondary standard and using only an unirradiated part for calibration.
Due to the uncertainties of the sample the accuracy of the absolute calibration is not assumed to be better than +-20%.
The error bars indicate the statistical errors that are practically neglegible (typically 0.1% of the data values).

<Gallery caption="ESRF ID01 PINHOLE data for C14" widths="300px" heights="200px">
Image:C14 ESRF ID01 PINHOLE.PNG
</Gallery>

Zip file of all data (in ASCII 3 column format) [[Media:GlassyCarbon_ESRF_ID01.zip|GlassyCarbon_ESRF_ID01.zip]]

===ESRF ID02 USAXS===

The calibration sample measured on ID02 is designated "Glassy Carbon type 2 C, sample C14", thickness 1 mm.
The scattering intensity has been calibrated with the USAXS camera relative to the primary beam without any
cross calibration.

Remark: To increase the resolution at very low q-values a third crystal is mounted perpendicular to the scanning crystals.
This reduces the sensitivity at higher q-values. Therefore only the range from qmin=0.0002*nm to qmax=0.06*nm has been measured.

<Gallery caption="ESRF ID02 USAXS data for C14" widths="300px" heights="200px">
Image:C14 ESRF ID02 USAXS.PNG
</Gallery>

Zip file of all data (in ASCII 3 column format) [[Media:GlassyCarbon_ESRF_ID02.zip|GlassyCarbon_ESRF_ID02.zip]]

=== Diamond I22 ===

canSAS - User contributions [en]

Glassy Carbon Round Robin